HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Iodophenylacetyl chloride → 4-[3-[(2-Iodophenylacetyl)amino]phenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Iodophenylacetyl chloride | HCID 10934858 | — |
| Reactant | 4-(3-Aminophenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione | HCID 86690010 | — |
| Product | 4-[3-[(2-Iodophenylacetyl)amino]phenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione | HCID 86690009 | 11% |
Reaction Steps
4-(3-Aminophenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione (30 mg, 0.1 mmol) and 2-iodophenylacetylchloride were used in a process similar to Example 9 to give the titled compound as a yellow crystal (6 mg, yield 11%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673915B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-fd91863711a74f5aa3192320e567c25c |
| Source note | uspto-grants-2014_03 |