HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzenesulfonyl chloride → HCID 86690021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| Reactant | HCID 86690022 | HCID 86690022 | — |
| Product | HCID 86690021 | HCID 86690021 | 46% |
Reaction Steps
4-(4-Aminophenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione hydrochloride (80 mg, 0.24 mmol) and 2-nitrobenzenesulfonyl chloride (78 mg, 0.35 mmol) were used in a process similar to Example 9 to give the titled compound (53 mg, yield 46%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673915B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-8573ca3aab0e47ebadd5e10dfdecc288 |
| Source note | uspto-grants-2014_03 |