HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86643474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 25001115 | HCID 25001115 | — |
| Product | HCID 86643474 | HCID 86643474 | 79% |
Reaction Steps
N-Methyl-5-((thiazol-2-ylamino)methyl)thiazol-2-amine (28 mg, 0.12 mmol) was dissolved in methanolic HCl (3 N, 1 mL) and Et2O was added. The precipitated solid was filtered by decantation and dried in vacuo, yielding N-methyl-5-((thiazol-2-ylamino)methyl)thiazol-2-amine dihydrochloride as a white solid (29 mg, 79%). Mp. 128-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673940B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-58f89f5b3761473b89d21608d1fc2d9a |
| Source note | uspto-grants-2014_03 |