HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenol → 2-Chlorophenyl pent-4-ynoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenol | HCID 7245 | — |
| Reactant | 4-Pentynoic acid | HCID 22464 | — |
| Product | 2-Chlorophenyl pent-4-ynoate | HCID 86086827 | 87.1% |
Reaction Steps
According to the protocol described in Example 235(B), the reaction between pent-4-ynoic acid (590 mg, 6.0 mmol) and 2-chlorophenol (771 mg, 6.0 mmol) afforded 1.09 g of 2-chlorophenyl pent-4-ynoate (Yield: 87%) as colorless-oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674106B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-7422e562b1b242879afbe881c4dcbf6c |
| Source note | uspto-grants-2014_03 |