Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | 4,5-Diamino-2-methyl-benzoic acid methyl ester | HCID 58575220 | — |
| Product | HCID 67133792 | HCID 67133792 | — |
Reaction Steps
A mixture of 3.98 g of methyl 4,5-diamino-2-methylbenzoate and 40 mL of diethyl oxalate was stirred at 145° C. for 3 hours. After cooling to room temperature, the solid was collected by filtration, washed with diethyl ether, and dried under reduced pressure to obtain 4.75 g of methyl 7-methyl-2,3-dioxo-1,2,3,4-tetrahydroquinoxaline-6-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08674096B2 |
|---|
| Source dataset | uspto-grants-2014_03 |
|---|
| ORD ID | ord-3df71f11c02f4646a2f9f52a8d942c27 |
|---|
| Source note | uspto-grants-2014_03 |
|---|
