HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Pentanoyloxy-5-nitrophenyl)-1-(4-methoxyphenyl)-ethanone → 1-Butyl-3-methyl-imidazolium valerate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Pentanoyloxy-5-nitrophenyl)-1-(4-methoxyphenyl)-ethanone | HCID 66688801 | — |
| Reactant | 1-Butyl-3-methylimidazolium Acetate | HCID 178476276 | — |
| Product | 1-Butyl-3-methyl-imidazolium valerate | HCID 178447536 | — |
Reaction Steps
The reaction was also carried out using 0.14 g (0.59 mmol) of the commercially available 1-butyl-3-methyl-imidazolium acetate with 0.11 g (0.29 mmol) of 2-(2-pentanoyloxy-5-nitrophenyl)-1-(4-methoxyphenyl)-ethanone (example 2) under the same reaction conditions as described in example 18. By comparing the LC-MS chromatogram of the crude reaction mixture with the chromatogram obtained from the reaction with 1-butyl-3-methyl-imidazolium valerate it was concluded that both methods delivered the targed compound in similar yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674121B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-64881362461c48688c40846f3ab466b4 |
| Source note | uspto-grants-2014_03 |