HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86666480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2-Chloro-4-fluoro-3-methyl-5-nitrobenzoic acid | HCID 10513831 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86666480 | HCID 86666480 | — |
Reaction Steps
A mixture of methylamine (2M THF solution, 8.56 mL, 17 mmol), 2-chloro-3-methyl-4-fluoro-5-nitro-benzoic acid (1.00 g, 4.2 mmol) and 20 mL THF is stirred over the weekend at rt. Then the mixture is acidified with 4M aq HCl and concentrated and the residue is washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674113B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-46e8bf2cb2f348248942264f95efac78 |
| Source note | uspto-grants-2014_03 |