HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86666484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2,3,4-Trifluoro-5-nitrobenzoic acid | HCID 15871241 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86666484 | HCID 86666484 | — |
Reaction Steps
A mixture of methylamine (40% aq solution, 0.68 mL, 6.7 mmol), 2,3,4-trifluoro-5-nitro-benzoic acid (0.50 g, 2.3 mmol) and 5 mL water is stirred for 3 h in an ice bath. Then the mixture is acidified with 6M aq HCl and the resulting precipitate is collected by filtration washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674113B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-4277a82d07a84988a2078956ec654e85 |
| Source note | uspto-grants-2014_03 |