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HRID1190309

反应详情

EQUATION

反应方程式

HRID 1190309 的结构方程式

REACTANTS

反应物

3
结构：NNCCO
HCID8017

2-Hydroxyethylhydrazine

C2H8N2O

结构：FC(F)(F)Cn1ncnc1-c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID58203849

8-Bromo-2-[2-(2,2,2-trifluoro-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene

C15H10BrF3N4OS

结构：NC(=O)c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID67050530

未命名化合物

PRODUCTS

生成物

1
结构：OCCn1ncnc1-c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID58204231

2-[5-(8-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulen-2-yl)-[1,2,4]triazol-1-yl]-ethanol

C15H13BrN4O2S

PROCEDURE

实验过程

Following the procedure for 8-Bromo-2-[2-(2,2,2-trifluoro-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene, 8-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid amide 25 was reacted with 2-hydrazino-ethanol to give 2-[5-(8-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulen-2-yl)-[1,2,4]triazol-1-yl]-ethanol. MS (ESI+) 393.0/395.0.