Tributyl Phosphate → Tbpa aeea

Participants

Reaction Steps

Reaction of TBPA with AEEA gives an TBPA/AEEA adduct. AEEA is sold in commerce by Dow Chemical. 43.6 mmol of TBPA was added to a round bottom flask with 51.00 grams of pure toluene. The mixture is heated to reflux after which 43.6 mmol of AEEA was added dropwise and the solution refluxed for one hour. The toluene is removed using a rotary evaporator to produce a yellow solid.

Provenance & Evidence