HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → HCID 131731253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | Tributyl Phosphate | HCID 31357 | — |
| Product | HCID 131731253 | HCID 131731253 | — |
Reaction Steps
Reaction of TBPA with AMPD gives an TBPA/AMPD adduct. AMPD is sold in commerce by Angus. 37.2 mmol of TBPA was combined with 37.2 mmol of AMPD in 164.5 g of pure ethanol. The mixture is refluxed for 2 hours. The solvent was removed using a rotary evaporator to produce a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08679990B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-50741cdd210a4d198527218adf03e46c |
| Source note | uspto-grants-2014_03 |