HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl piperazine-1-carboxylate → HCID 84103730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | 2,4-Dichloro-3-nitropyridine | HCID 10535773 | — |
| Product | HCID 84103730 | HCID 84103730 | 94.7% |
Reaction Steps
The specific operation referred to the step (1) described in Example 1 for details. 2,4-dichloro-3-nitropyridine (772 mg, 4.0 mmol), and piperazine-1-carboxylic acid tert-butyl ester (744 mg, 4.0 mmol) were charged to afford 1.299 g crude product with a yield of 94.7%, which was directly used in the subsequent reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680089B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-aae41e8f91074ffe92a54aab541b8c6d |
| Source note | uspto-grants-2014_03 |