17551-00-7 → HCID 86707738, compound

Participants

Reaction Steps

Compound 90e was prepared from Compound 90d and 2-sulfamoylacetic acid using the procedure given for Compound 1b. LCMS=1.78 min using analytical method (Q), 405.1 (M+H). 1H NMR (500 MHz, CD3OD) δ 8.07 (d, J=1.7 Hz, 1H), 7.74-7.67 (m, 2H), 7.56 (dd, J=12.0, 1.5 Hz, 1H), 7.52-7.43 (m, 2H), 7.43-7.36 (m, 1H), 4.94-4.88 (m, 2H), 4.78-4.74 (m, 2H).

Provenance & Evidence