HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 28343695, compound → HCID 58495679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 28343695 | HCID 28343695 | — |
| Reactant | 7-Chloro-3-(2,2,2-trifluoroacetyl)-6-trifluoromethylsulfonyloxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine | HCID 57447747 | — |
| Product | HCID 58495679 | HCID 58495679 | 45% |
Reaction Steps
Use a method similar to the General Procedure 1-3, using 7-chloro-3-(2,2,2-trifluoroacetyl)-6-trifluoromethanesulfonyloxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine (175 mg, 0.42 mmol) and 4-(3-methyl-butyryl)-benzylamine (160 mg, 0.8 mmol) to obtain the title compound as a yellow syrup (85 mg, 45%). MS (ES+) m/z: 467 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680091B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-ee37b6d525b64089b3343a67d4bc3f01 |
| Source note | uspto-grants-2014_03 |