Hydrochloric Acid → HCID 67463701, compound

Participants

Reaction Steps

Add 4N hydrogen chloride in dioxane (10.5 mL) to a solution of N-(tert-butoxycarbonyl)-4-(2-methylamino-oxazol-4-yl)-benzylamine (624 mg, 1.6 mmol) in DCM (250 mL). Stir the solution at room temperature for 16 h in a sealed flask. Concentrate the mixture in vacuo to a solid. Slurry the solid in excess of diethyl ether and filter. Collect the white solid to obtain the title compound (1.48 g, 95%). MS (ES+) m/z: 204.1 (M+H)+.

Provenance & Evidence