Succinic Acid → HCID 67465071, compound

Participants

Reaction Steps

Dissolve 7-chloro-6-{4-[(N-methyl-iso-propylamino)-methyl]-benzylamino}-2,3,4,5-tetrahydro-1H-benzo[d]azepine (250 mg, 0.67 mmol) in methanol and add succinic acid (75 mg, 0.63 mmol). Stir the mixture until homogeneous. Concentrate the mixture in vacuo, dissolve in water, and freeze dry the solution to obtain the title compound (325 mg, 95%). MS (APCI+) m/z: 372 (M+H)+.

Provenance & Evidence