Succinic Acid → HCID 67463174, compound

Participants

Reaction Steps

Dissolve 7-chloro-6-[4-(2,2-dimethyl-propanesulfonylmethyl)-benzylamino]-2,3,4,5-tetrahydro-1H-benzo[d]azepine (316 mg, 0.726 mmol) in methanol (10 mL) and add succinic acid (86 mg, 0.726 mmol). Stir the mixture for 2 h. Concentrate the mixture in vacuo and dry under high vacuum at 50° C. to obtain the title compound (380 mg, 94%). MS (APCI+) m/z: 435 (M+H)+.

Provenance & Evidence