Hydrazine hydrate (1:1) → HCID 86634373, compound

Participants

Reaction Steps

To a solution of the compound 6 (493 mg) in methanol (13 mL), hydrazine monohydrate (339 mg) was added. The reaction mixture was stirred at room temperature for overnight. The reaction mixture was concentrated and then added dichloromethane. The appeared solid was collected by filtration and then the residue was concentrated and obtained the title compound (245 mg) having the following physical properties.

Provenance & Evidence