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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1191276Generated: October 31, 2026

HCID 86634375, compound → HCID 11848418, compound

https://huagongshe.com/reaction/1191276

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86634375HCID 86634375—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 11848418HCID 1184841899.3%

Reaction Steps

In a solution of the compound 9 (125 mg) in ethanol (4 mL), 10% palladium carbon (wet, 112 mg) was added under an argon atmosphere. The reaction mixture was stirred under a hydrogen atmosphere at room temperature for 30 minutes. The reaction mixture was filtered with Celite (trade name) and the filtrate was concentrated and obtained the title compound (116 mg) having the following physical properties.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08680092B2
Source datasetuspto-grants-2014_03
ORD IDord-3cbfe8979af6404491aa12d0b3154938
Source noteuspto-grants-2014_03