HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86634375, compound → HCID 11848418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86634375 | HCID 86634375 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11848418 | HCID 11848418 | 99.3% |
Reaction Steps
In a solution of the compound 9 (125 mg) in ethanol (4 mL), 10% palladium carbon (wet, 112 mg) was added under an argon atmosphere. The reaction mixture was stirred under a hydrogen atmosphere at room temperature for 30 minutes. The reaction mixture was filtered with Celite (trade name) and the filtrate was concentrated and obtained the title compound (116 mg) having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680092B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-3cbfe8979af6404491aa12d0b3154938 |
| Source note | uspto-grants-2014_03 |