HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 86634378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 86634377 | HCID 86634377 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86634378 | HCID 86634378 | — |
Reaction Steps
The compound 15 (125 mg), methanol (0.5 mL) and 4N hydrogen chloride-dioxane solution (2 mL) were stirred at room temperature for 1 hour. The reaction solution was concentrated and obtained the title compound (118 mg) having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680092B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-588d4fe3a30d455fb5e89c8d77cf20a9 |
| Source note | uspto-grants-2014_03 |