HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 11848560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 86634385 | HCID 86634385 | — |
| Product | HCID 11848560 | HCID 11848560 | 87% |
Reaction Steps
The compound 21 (102 mg) and 10% hydrogen chloride-methanol solution (2 mL) were stirred at room temperature for 5 hours. The reaction solution was concentrated, added aqueous 2N sodium hydroxide solution and then extracted with dichloromethane. The extract was dried over anhydrous magnesium sulfate, concentrated and obtained the title compound (71 mg) having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680092B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-00760a7f43d4492cb17b3602af8eb3de |
| Source note | uspto-grants-2014_03 |