HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1191296Generated: November 1, 2026
HCID 68916161, compound → HCID 68918306, compound
https://huagongshe.com/reaction/1191296
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 68916161 | HCID 68916161 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Product | HCID 68918306 | HCID 68918306 | — |
Reaction Steps
To a solution of the compound 42 in methanol (2 mL), hydrazine monohydrate (98%, 19.5 μL) was added and stirred at 40° C. for overnight. The reaction solution was concentrated and purified by thin-layer chromatography to obtain the title compound (21.4 mg) having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08680092B2 |
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| Source dataset | uspto-grants-2014_03 |
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| ORD ID | ord-a244fffbee60425b828dbfa027369027 |
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| Source note | uspto-grants-2014_03 |
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