HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56651010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 56651011 | HCID 56651011 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 56651010 | HCID 56651010 | 100% |
Reaction Steps
To a solution of 4-(3-aminophenyl)-1H-benzo[h]quinazolin-2-one (25 mg, 0.087 mmol) in chloroform (2 mL)/methanol (1 mL) was added a solution of 4M hydrogen chloride in ethyl acetate (1 mL), and stirred for 1 hour. The solvent was removed under reduced pressure to give the titled compound as a orange powder (30 mg, yield 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680110B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-a805d2298899426bb3e41325669db506 |
| Source note | uspto-grants-2014_03 |