2-Phenoxyethanamine → HCID 46932519, compound

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Reaction Steps

Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (100 mg, 0.28 mmol) and 2-Phenoxy ethylamine (45 mg, 0.32 mmol). The title compound was obtained as a solid (32 mg, 24% yield). 1H NMR (400 MHz, d6-DMSO) δ: 9.11 (1H, m), 8.99 (2H, m), 8.47 (1H, s), 7.27 (2H, m), 6.93 (3H, m), 4.04 (2H, m), 3.56 (2H, m). MS m/z: 468.03, 470.03 [M+H]+.

Provenance & Evidence