Methyl 4-(aminomethyl)benzoate hydrochloride → HCID 60207391, compound

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Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carbonyl chloride (120 mg, 0.33 mmol) and methyl 4-(aminomethyl)benzoate hydrogen chloride (81 mg, 0.39 mmol). The title compound was obtained as a solid (70 mg, 35% yield). 1H NMR (400 MHz, d6-DMSO) δ: 9.46 (1H, m), 8.98 (2H, s), 8.48 (1H, s), 7.91 (2H, m), 7.43 (2H, m), 4.49 (2H, m), 3.84 (3H, s). MS m/z: 496.31, 498.15 [M+H]+.

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