HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzylamine → HCID 60207393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzylamine | HCID 97472 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Product | HCID 60207393 | HCID 60207393 | — |
Reaction Steps
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and 4-hydroxylbenzylamine (14.5 mg, 0.12 mmol). The title compound was obtained as a solid (23.1 mg, 51% yield). MS m/z: 455.96, 457.96 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-f2def09da5b74874b5a9d6d0a3939f94 |
| Source note | uspto-grants-2014_03 |