HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[2-(Dimethylamino)ethyl]-3-methyl-1H-pyrazol-5-amine → HCID 60207406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[2-(Dimethylamino)ethyl]-3-methyl-1H-pyrazol-5-amine | HCID 2758501 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Product | HCID 60207406 | HCID 60207406 | — |
Reaction Steps
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and 1-(2-(dimethylamino)ethyl)-3-methyl-1H-pyrazol-5-amine (17.0 mg, 0.10 mmol). The title compound was obtained as a solid (20.8 mg, 23% yield). MS m/z: 501.02, 503.02 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-07ccb6ceaa6f40f8a5093c1a4c01e6a4 |
| Source note | uspto-grants-2014_03 |