HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[2-(Dimethylamino)ethoxy]aniline → HCID 60207416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[2-(Dimethylamino)ethoxy]aniline | HCID 6484655 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Product | HCID 60207416 | HCID 60207416 | — |
Reaction Steps
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and 4-(2-(dimethylamino)ethoxy)aniline (17.0 mg, 0.12 mmol). The title compound was obtained as a solid (17.5 mg, 34% yield). MS m/z: 513.02, 515.02 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-51b0bcec4e4a4eb3a0c0a0c58d9d6949 |
| Source note | uspto-grants-2014_03 |