HuagongsheHuagongshe Chemistry Print Report · For research reference only
N~3~,N~3~-Dimethyl-1-phenylpropane-1,3-diamine → HCID 60207426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N~3~,N~3~-Dimethyl-1-phenylpropane-1,3-diamine | HCID 25248080 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Product | HCID 60207426 | HCID 60207426 | — |
Reaction Steps
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and N1,N1-dimethyl-3-phenylpropane-1,3-diamine (17.8 mg, 0.1 mmol). The title compound was obtained as a solid (15.8 mg, 31% yield). MS m/z: 510.89, 513.89 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-572cadbb8d1d47ddb70cb62dae010d05 |
| Source note | uspto-grants-2014_03 |