HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Aminopropoxy)(tert-butyl)dimethylsilane → HCID 60207448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Aminopropoxy)(tert-butyl)dimethylsilane | HCID 11074190 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Product | HCID 60207448 | HCID 60207448 | — |
Reaction Steps
Prepared according to the procedure described for example 70 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (1.5 g, 4.3 mmol) and 3-(tert-butyl(dimethyl)silyl)oxypropan-1-amine (0.98 g, 5.12 mmol). The title compound was obtained as a yellow solid (1.1 g, 49% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-d0dc248671554950917bf23198554af1 |
| Source note | uspto-grants-2014_03 |