HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid → HCID 178439393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| Reactant | HCID 178439404 | HCID 178439404 | — |
| Product | HCID 178439393 | HCID 178439393 | — |
Reaction Steps
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and 3-isopropyl-1H-pyrazol-5-amine (12.5 mg, 0.1 mmol). The title compound was obtained as a solid (7.1 mg, 16% yield). MS m/z: 458.00, 460.00 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-fc42d1df16c641cebeed6b282f1c3244 |
| Source note | uspto-grants-2014_03 |