Dodecylamine → HCID 86676425, compound

Participants

Reaction Steps

Diethyl 2,2′-(hexane-1,6-diylbis(azanediyl))bis(2-oxoacetate) (5.00 g, 15.8 mmol) and dodecyl amine (5.85 g, 31.64 mmol) were dissolved in 100 ml of CHCl3. Subsequently the mixture was heated at reflux temperature for 24 hours. The solvent was removed by filtering the product. The remaining solid was washed two times with CHCl3 and two times with diethyl ether and dried in vacuum. The product was obtained as a white powder.

Provenance & Evidence