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HRID1192528

反应详情

EQUATION

反应方程式

HRID 1192528 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1cc(F)cc(F)c1
HCID2734338

3,5-Difluorophenylboronic acid

C6H5BF2O2

结构：COC(=O)c1cc(Cl)c(C#C[Si](C)(C)C)c([N+](=O)[O-])c1OS(=O)(=O)C(F)(F)F
HCID58368634

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(Cl)c(C#C[Si](C)(C)C)c([N+](=O)[O-])c1-c1cc(F)cc(F)c1
HCID58368637

未命名化合物

收率 82%

PROCEDURE

实验过程

The desired compound was prepared according to the procedure of Example 16, step E, using methyl 5-chloro-3-nitro-2-{[(trifluoromethyl)sulfonyl]oxy}-4-[(trimethylsilyl)ethynyl]benzoate and (3,5-difluorophenyl)boronic acid as the starting materials in 82% yield. LCMS for C19H17ClF2NO4Si (M+H)+: m/z=424.1; Found: 423.9.