HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Difluorophenyl)boronic acid → HCID 58368637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Difluorophenyl)boronic acid | HCID 2734338 | — |
| Reactant | HCID 58368634 | HCID 58368634 | — |
| Product | HCID 58368637 | HCID 58368637 | 82% |
Reaction Steps
The desired compound was prepared according to the procedure of Example 16, step E, using methyl 5-chloro-3-nitro-2-{[(trifluoromethyl)sulfonyl]oxy}-4-[(trimethylsilyl)ethynyl]benzoate and (3,5-difluorophenyl)boronic acid as the starting materials in 82% yield. LCMS for C19H17ClF2NO4Si (M+H)+: m/z=424.1; Found: 423.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680108B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-d85a203e2e5a4c4c99cc1a3f324f5aa1 |
| Source note | uspto-grants-2014_03 |