HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 66864588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 66865144 | HCID 66865144 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66864588 | HCID 66864588 | — |
Reaction Steps
To a solution of ethyl 2-(1-methyl-3-(4-pentylphenylsulfonamido)pyrrolidin-3-yl)acetate (25 mg, 0.063 mmol) in methylene chloride (1 mL) was added methyl iodide (100 μL). The solution was stirred overnight and concentrated to give the title compound as a white solid (33 mg, quantitative). ESI 411.3 [M]+, calcd for [C21H35N2O4S]+ 411.23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680282B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-561e003c6d74447eb9d6c1002992b0a7 |
| Source note | uspto-grants-2014_03 |