HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 131731272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Trimethyl[(3-methylpent-1-yn-3-yl)oxy]silane | HCID 15581391 | — |
| Reactant | HCID 131731273 | HCID 131731273 | — |
| Product | HCID 131731272 | HCID 131731272 | — |
Reaction Steps
As in reaction conditions of Example XIX Step 1, to 3.29 mL of toluene, the 0.02 g carbonylchlorohydridebis(tricyclohexylphosphine)ruthenium(H) was added, and the reaction was carried out between 1.64 g 1,2-bis(dimethylvinylsilyl)ethane and 0.47 g 3-methyl-3-(trimethylsiloxy)pent-1-yne. Raw 1-{[3-methyl-3-(trim ethyl siloxy)-1-pentynyl]dimethylsilyl}-2-(dimethylvinylsilyl)ethane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680310B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-c4216357105e40bf9252fabcea15fa30 |
| Source note | uspto-grants-2014_03 |