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HRID1192983

反应详情

EQUATION

反应方程式

HRID 1192983 的结构方程式

REACTANTS

反应物

3
反应SMILES：Cc1ccccc1
HCID1140

Toluene

C7H8

反应SMILES：C=C[Si](C)(C)N[Si](C)(C)C=C
HCID82126

Silanamine, 1-ethenyl-N-(ethenyldimethylsilyl)-1,1-dimethyl-

C8H19NSi2

反应SMILES：C#CC1(O[Si](C)(C)C)CCCCC1
HCID552482

Silane, [(1-ethynylcyclohexyl)oxy]trimethyl-

C11H20OSi

PRODUCTS

产物

1
反应SMILES：C=C[Si](C)(C)N[Si](C)(C)C1(C#CO[Si](C)(C)C)CCCCC1
HCID67034799

未命名化合物

PROCEDURE

实验过程

As in reaction conditions of Example XIX Step 1, to 4.69 mL of toluene, the 0.02 g carbonylchlorohydridebis(triisopropylphosphine)ruthenium(II) was added, and the reaction was carried out between 2.29 g 1,1,3,3-tetramethyl-1,3-divinyldisilazane and 0.81 g 1-ethynyl-1-(trimethylsiloxy)cyclohexane. Raw 1-[(1-trimethylsiloxy-1-ethynyl)cyclohexyl]-1,1,3,3-tetramethyl-3-vinyldisilazane was obtained.

WORKUP

后处理

  1. customAs in reaction conditions of Example XIX Step 1