HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 67034799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 1,1,3,3-Tetramethyl-1,3-divinyldisilazane | HCID 82126 | — |
| Reactant | Silane, [(1-ethynylcyclohexyl)oxy]trimethyl- | HCID 552482 | — |
| Product | HCID 67034799 | HCID 67034799 | — |
Reaction Steps
As in reaction conditions of Example XIX Step 1, to 4.69 mL of toluene, the 0.02 g carbonylchlorohydridebis(triisopropylphosphine)ruthenium(II) was added, and the reaction was carried out between 2.29 g 1,1,3,3-tetramethyl-1,3-divinyldisilazane and 0.81 g 1-ethynyl-1-(trimethylsiloxy)cyclohexane. Raw 1-[(1-trimethylsiloxy-1-ethynyl)cyclohexyl]-1,1,3,3-tetramethyl-3-vinyldisilazane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680310B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-47fd03e2b644441db30c1bc31c918779 |
| Source note | uspto-grants-2014_03 |