HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Heptyne → HCID 86667904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Heptyne | HCID 12350 | — |
| Reactant | 1,3-Divinyltetramethyldisiloxane | HCID 75819 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86667904 | HCID 86667904 | — |
Reaction Steps
As in reaction conditions of Example XIX Step 1, to 6.25 mL of toluene, the 0.05 g carbonylchlorohydridebis(triisopropylphosphine)ruthenium(II) was added, and the reaction was carried out between 2.87 g 1,1,3,3-tetramethyl-1,3-divinyldisiloxane and 0.49 g 1-heptyne. Raw 1-(1-heptynyl)-1,1,3,3-tetramethyl-3-vinyldisiloxane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680310B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-31fed6c976684ba0aa914d9cadcaa1f3 |
| Source note | uspto-grants-2014_03 |