HRID1192985

反应详情

EQUATION

反应方程式

HRID 1192985 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

As in reaction conditions of Example XIX Step 1, to 6.25 mL of toluene, the 0.05 g carbonylchlorohydridebis(triisopropylphosphine)ruthenium(II) was added, and the reaction was carried out between 2.87 g 1,1,3,3-tetramethyl-1,3-divinyldisiloxane and 0.49 g 1-heptyne. Raw 1-(1-heptynyl)-1,1,3,3-tetramethyl-3-vinyldisiloxane was obtained.

WORKUP

后处理

  1. customAs in reaction conditions of Example XIX Step 1