HRID1193019

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID170903

Pentanal, 5,5-dimethoxy-

C7H14O3

HCID11469495

1-(4-CHLOROPHENYL)-2-NITROETHANE

C8H8ClNO2

PRODUCTS

生成物

$结构：O=CCCC/C=C(\Cc1ccc(Cl)cc1)[N+](=O)[O-]$

HCID25187598

未命名化合物

收率 45.1%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Prepared according to the general procedure B from 1-chloro-4-(2-nitroethyl)benzene 112g (24 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.93 g, 45% yield) after silica gel chromatography (EtOAc/Hexane).

WORKUP

后处理

customPrepared