HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-iodobenzoic acid → 2-(2H-1,2,3-Triazol-2-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| Reactant | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| Product | 2-(2H-1,2,3-Triazol-2-yl)benzoic acid | HCID 21313592 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Intermediate 13, substituting 2-iodo-benzoic acid for 5-fluoro-2-iodo-benzoic acid. 1H NMR (400 MHz, CD3OD): 7.91 (s, 2H), 7.85-7.82 (m, 1H), 7.75 (dd, J=8.1, 1.0 Hz, 1H), 7.69 (td, J=7.7, 1.5 Hz, 1H), 7.60-7.55 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680275B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-68dce9a6e2c3497f934df72ee00a9e7f |
| Source note | uspto-grants-2014_03 |