HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 67086519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 3-Fluorophthalic anhydride | HCID 69551 | — |
| Product | HCID 67086519 | HCID 67086519 | — |
Reaction Steps
3-Fluorophthalic anhydride (377 mg, 2.27 mmol) was dissolved in MeOH (6 mL) and heated to reflux for 15 h. The mixture was concentrated in vacuo and the two products (400 mg, 89%), 2-fluoro-6-(methoxycarbonyl)benzoic acid and 3-fluoro-2-(methoxycarbonyl)benzoic acid, were taken on to the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680275B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-b2cdc1a0204140329e635c505aa258b2 |
| Source note | uspto-grants-2014_03 |