HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotrimethylsilane → HCID 86742782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 86742783 | HCID 86742783 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86742782 | HCID 86742782 | — |
Reaction Steps
Tetramethyl 2-benzylthioethane-1,1-diphosphonate (2.45 g) in chloroform (5 cm3) was treated with an excess of trimethylsilyl bromide (5.1 g) at room temperature. The formation of the trimethylsilyl esters was monitored by 31P n.m.r. and was complete after 15 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810486 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-1325b4ff41e748d9bee54fcbddd1993a |
| Source note | uspto-grants-1989_03 |