HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21272305, compound → HCID 21272366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21272305 | HCID 21272305 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21272366 | HCID 21272366 | 92% |
Reaction Steps
Ethyl 4-[3-(4-methoxyphenylamino)-1H-pyrazol-1-yl]phenoxyacetate (1.0 g) in ethanol (200 ml) and 10% sodium hydroxide (5 ml) was heated to reflux for 1 hour. Upon cooling, the resultant pink solid was filtered off and treated with a little 10% hydrochloric acid to give a violet solid which was filtered off, rinsed with water and dried to give the title compound (0.85 g), mp 163°-165°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810719 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-1cf55d9e3da6434897c99ce88cdbd115 |
| Source note | uspto-grants-1989_03 |