Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 21272324 | HCID 21272324 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21272298 | HCID 21272298 | 85.7% |
Reaction Steps
A mixture of 4-(1-phenyl-1H-pyrazol-3-yl)aminophenol (2.0 g), acetic anhydride (4 g) and sulphuric acid (0.2 g) was heated at 100° C. on the steam bath for 15 minutes, water was added and the product was collected by filtration and dried to give the sub-title compound (2.0 g) as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04810719 |
|---|
| Source dataset | uspto-grants-1989_03 |
|---|
| ORD ID | ord-c7b934a42c4a48df9b962b340b27a5ae |
|---|
| Source note | uspto-grants-1989_03 |
|---|
