HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroacetate → HCID 21272323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroacetate | HCID 7751 | — |
| Reactant | HCID 21272346 | HCID 21272346 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21272323 | HCID 21272323 | — |
Reaction Steps
A solution of N-(1-phenyl-1H-pyrazol-3-yl)thiourea (4.2 g) and ethyl 2-chloroethanoate (3.0 g) in ethyl alcohol (50 ml) was heated under reflux for 2 hours. The mixture was cooled and the title compound collected by filtration as a yellow solid 4.0 g, mp >230°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810719 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-fccf0ea7eff1459cbc059a37ff6cc01c |
| Source note | uspto-grants-1989_03 |