HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178493620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178493616 | HCID 178493616 | — |
| Product | HCID 178493620 | HCID 178493620 | — |
Reaction Steps
200 mg. (0.56 mmol) 7,7-dimethyl-2-(2-methoxy-4-methylthiophenyl)-6,7-dihydro-3H,5H-pyrrolo[2,3-f]-benzimidazol-6-one were stirred for 48 hours at ambient temperature in 4 ml. glacial acetic acid and 0.4 ml. 30% hydrogen peroxide. 10 ml. water were added thereto and the solvent was removed in a vacuum. There were obtained 160 mg. (75% of theory) of the title compound which, after crystallization from ethanol, had a melting point of 235°-237° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810801 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-bc7cf620eb8d4220b0ed53d0a01b6226 |
| Source note | uspto-grants-1989_03 |