Methyl iodide → HCID 14049927, compound

HRID 1193592Notes

Reaction equation

HRID 1193592 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH2:8])=[CH:5][CH:4]=1.[C:11](=[S:13])=[S:12].I[CH3:15]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:8][C:11](=[S:13])[S:12][CH3:15])=[CH:5][CH:4]=1

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 6348Carbon DisulfideHCID 754524-Methoxybenzylamine

Product 1

HCID 14049927HCID 14049927, compound

Procedure

4-Methoxybenzylamine (0.073 mol) was reacted with carbon disulfide (0.073 mol) and iodomethane (0.073 mol) substantially as described in Example 1B above to obtain 7.2 g (43%) as a crystalline solid: mp 67°-70°.

Workup

  1. customto obtain 7.2 g (43%) as a crystalline solid

Sources & evidence

ORD record
ord-3a39db53d0754f898d1ef59ef4cf6274
Source dataset
uspto-grants-1989_03
Patent number
US04810811

Reaction notes

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