HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Chloropropoxy)-4-fluorobenzene → HCID 14407087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Chloropropoxy)-4-fluorobenzene | HCID 74391 | — |
| Reactant | 4-[Bis(4-fluorophenyl)methyl]piperidine | HCID 13250544 | — |
| Product | HCID 14407087 | HCID 14407087 | 53% |
Reaction Steps
Following the combined procedures of Examples 14 and 16, 4-[bis(4-fluorophenyl)methyl]piperidine and 4-(3-chloropropoxy)-1-fluorobenzene were reacted and worked up by chromatography in Example 16, to give the free base in 53% yield as a yellow oil after drying in vacuo at 80° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810713 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-c3748be4a5c448a29e5453ea5bc20e17 |
| Source note | uspto-grants-1989_03 |